HRID1091097

反应详情

EQUATION

反应方程式

HRID 1091097 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

N-Methyl-6-nitro-N-[(4-nitrophenoxy)propyl]-2-quinoline methanamine (2.60 g, 6.57 mmol) was dissolved in ethanol (170 mL) containing PtO2 (0.39 g). The mixture was charged with H2 (g) (1 atm), stirred for 4 hours, and filtered through a pad of solka floc. The filtrate was concentrated to afford 2.18 g of product as a yellow oil that was used directly without purification.

WORKUP

后处理

  1. additionThe mixture was charged with H2 (g) (1 atm)
  2. filtrationfiltered through a pad of solka floc
  3. concentrationThe filtrate was concentrated