HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 20818712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 20818713 | HCID 20818713 | — |
| Product | HCID 20818712 | HCID 20818712 | — |
Reaction Steps
Cis-4-tert-butoxycarbonyl-3,5-dimethylmorpholine g, 8.18 mmol) was dissolved in 4N-hydrochloric acid/1,4-dioxane (50 mL), and the solution was stirred for 3 days at room temperature. The reaction liquor was concentrated under reduced pressure and dried, to obtain the title compound as an oily matter. This compound was used in the subsequent reaction without performing further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129366B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-cc9905dbfa404b7187cd27cc1a476058 |
| Source note | uspto-grants-2012_03 |