HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 11627685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 55280267 | HCID 55280267 | — |
| Reactant | HCID 86624651 | HCID 86624651 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11627685 | HCID 11627685 | — |
Reaction Steps
To a solution of 4-[4-(pentafluoroethoxy)phenoxy]piperidine hydrochloride (0.17 g) and diisopropylethylamine (0.19 mL) in dichloromethane (100 mL) was added [(4S)-4-ethyl-2,5-dioxoimidazolidin-4-yl]methanesulfonyl chloride (0.13 g). The reaction was stirred at ambient temperature for 18 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129412B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-9f00ab9de53f45cf8941d22378b2b94d |
| Source note | uspto-grants-2012_03 |