HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 53629097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | 1-(Ethylamino)cyclopentane-1-carbonitrile | HCID 21678969 | — |
| Product | HCID 53629097 | HCID 53629097 | — |
Reaction Steps
This material was obtained in analogy to example 65 step a, from 1-ethylamino-cyclopentanecarbonitrile (7.5 g), synthesis described in: J. Med. Chem.; 1969; 473, by reduction with diisobutylaluminiumhydride (20% in toluene, 282.6 mL) as an oil (6.55 g) and directly used in the next reaction step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129423B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-5b45265580664c37b71fb8a29339d42b |
| Source note | uspto-grants-2012_03 |