HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(aminomethyl)-N,N-dibenzyloxetan-3-amine → 3-(aminomethyl)-N-benzyloxetan-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(aminomethyl)-N,N-dibenzyloxetan-3-amine | HCID 57415821 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(aminomethyl)-N-benzyloxetan-3-amine | HCID 57415855 | — |
Reaction Steps
To (3-Aminomethyl-oxetan-3-yl)-dibenzyl-amine in methanol (10 ml) was added a catalytic amount of 10% Pd/C and the reaction mixture was then stirred at RT under an atmosphere of H2 for 8 h. The catalyst was removed by filtration, the filtrate concentrated under reduced pressure to provide the title compound (90 mg) as colorless oil, MS (EI): 192 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129423B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-fa9cd0f963544b26b95f936a2f01a27f |
| Source note | uspto-grants-2012_03 |