Triethylamine → HCID 66593908, compound

HRID 1092466Notes

Reaction equation

HRID 1092466 reaction equation
[CH3:1][C:2]1[CH:6]([CH3:7])[CH:5]=[C:4]([CH3:8])[C:3]=1[C:9]1[CH:14]=[C:13]([CH3:15])[CH:12]=[C:11]([CH3:16])[C:10]=1[NH2:17].C(N(CC)CC)C.[C:25](Cl)(=[O:30])[C:26]([CH3:29])([CH3:28])[CH3:27]>>[CH3:1][C:2]1[CH:6]([CH3:7])[CH:5]=[C:4]([CH3:8])[C:3]=1[C:9]1[CH:14]=[C:13]([CH3:15])[CH:12]=[C:11]([CH3:16])[C:10]=1[NH:17][C:25](=[O:30])[C:26]([CH3:29])([CH3:28])[CH3:27]

Participants

4

Reactant 3

HCID 8471TriethylamineHCID 62493Pivaloyl chlorideHCID 66593770HCID 66593770, compound

Product 1

HCID 66593908HCID 66593908, compound

Procedure

The same experiment as in Example 49 was performed using 0.600 g (2.64 mmol) of 2-(2,3,5-trimethylcyclopenta-1,4-dienyl)-4,6-dimethylphenylamine, 0.321 g (3.17 mmol) of triethylamine, and 0.382 g (3.17 mmol) of pivaloyl chloride (0.727 g, 89%).

Sources & evidence

ORD record
ord-9ef2d0b5114944afaf73d8ee86fb650e
Source dataset
uspto-grants-2012_03
Patent number
US08129488B2

Reaction notes

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