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HRID1092571

反应详情

EQUATION

反应方程式

HRID 1092571 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)C[C@@H](C(=O)OC(C)(C)C)N1CCCS1(=O)=O
HCID66590788

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)C[C@@H](C(=O)O)N1CCCS1(=O)=O
HCID28166009

未命名化合物

PROCEDURE

实验过程

tert-Butyl(2S)-2-(1,1-dioxidoisothiazolidin-2-yl)-4-methylpentanoate (0.656 g, 2.251 mmol) from Step B was combined with HCl (4 N in dioxane, 5 mL, 20.00 mmol). The reaction mixture was stirred at room temperature for 24 hours, then the solvent removed in vacuo to furnish (2S)-2-(1,1-dioxidoisothiazolidin-2-yl)-4-methylpentanoic acid: MS (DCI+) m/z 253 (M+NH4)+.

WORKUP

后处理

  1. customthe solvent removed in vacuo