Hydrogen Bromide → HCID 66588691, compound

Participants

Reaction Conditions

Reaction Steps

Intermediate III (16 mg) was placed in a microwave reactor vial and 48% HBr (1 mL) was added. The reactor was sealed, and the mixture was stirred at 170° C. for 1 h under microwave irradiation. The precipitated product was filtered off and dried in vacuo. Yield of example 2a2: 11 mg as a solid. LC/MS (method 17): RT 1.27 min, ELSD 88%, UV 75.1%, MH+: 220.1.

Provenance & Evidence