HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → HCID 66590094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | 2-Chloro-3,6-difluorophenol | HCID 2773561 | — |
| Product | HCID 66590094 | HCID 66590094 | 31% |
Reaction Steps
2-Chloro-3,6-difluorophenol was reacted with 1,2-dibromoethane according to the procedure described in Step 2A to yield 2C (2.1 g, 31%). 1H NMR (400 MHz, CHLOROFORM-d) δ ppm 3.65 (t, J=6.57 Hz, 2H), 4.43 (t, J=6.57 Hz, 2H) 6.89 (m, 1H) 7.01 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129538B1 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-34757d213564454eaaf7a468328ec5a8 |
| Source note | uspto-grants-2012_03 |