HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 86761505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Ethylhydrazine | HCID 29062 | — |
| Reactant | 8-Oxa-3-azabicyclo[3.2.1]octane | HCID 12069231 | — |
| Reactant | HCID 75080606 | HCID 75080606 | — |
| Product | HCID 86761505 | HCID 86761505 | — |
Reaction Steps
A procedure similar to that used for the synthesis of 3-(1-(1-benzylpiperidin-4-yl)-6-chloro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)-8-oxa-3-azabicyclo[3.2.1]octane is used, using ethyl hydrazine as the hydrazine component and substituting 3-oxa-8-azabicyclo[3.2.1]octane for 8-oxa-3-azabicyclo[3.2.1]octane. (65%, MS=294.3 (M+H))
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129371B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-23505efbec57439a80cc7f7692f77014 |
| Source note | uspto-grants-2012_03 |