Hydrochloric Acid → HCID 66594027, compound

Participants

Reaction Conditions

Reaction Steps

Compound 102-3 (550 mg) was dissolved in ethanol (18 ml), concentrated hydrochloric acid (3.5 ml) was added, and the mixture was stirred at 50° C. for 4 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether and methanol to give the object product (180 mg) as a white powder.

Provenance & Evidence