HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → HCID 86618174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | tert-Butyl acrylate | HCID 15458 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86618174 | HCID 86618174 | 88% |
Reaction Steps
To acetone (50 g) were dissolved t-butylacrylate (5.0 g), methacrylic acid (2.0 g), methyl methacrylate (3.0 g) and AIBN (2,2′-azobisisobutyronitrile) (0.02 g) as a polymerization initiator, and then the resulting mixture was polymerized at about 67° C. for about 6 hours. After polymerization is completed, the resulting mixture was filtered and vacuum dried to obtain poly(t-butylacrylate/methacrylic acid/methyl methacrylate) (yield: 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133547B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-ce37410fa5bc433d8e54364e4d20b495 |
| Source note | uspto-grants-2012_03 |