HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 72581644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 69152767 | HCID 69152767 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 72581644 | HCID 72581644 | — |
Reaction Steps
2.00 g (4.97 mmol) of (6aR*,10aR*)-1-(tert-butyldimethylsilyloxy)-3-pentyl-6a,7,8,9,10,10a-hexahydrobenzo[c]chromen-6-one was heated under reflux at 140° C. for 17 h with 4.25 g (10.2 mmol) of Lawesson's reagent in xylene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133887B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-06c5c7974da642a6a2119e7650901676 |
| Source note | uspto-grants-2012_03 |