(3-Bromopropyl)benzene → HCID 25115525, compound

Participants

Reaction Steps

The synthesis of title compounds started from Compound 70a and (3-bromopropyl)benzene, according to procedures described in the synthesis of Compound 70. 1H NMR (400 MHz, CHLOROFORM-d) δ ppm 2.41-2.53 (m, 2H) 3.16 (m, 2H) 3.68 (s, 3H) 3.77-3.83 (m, 2H) 3.96 (s, 3H) 4.16 (s, 3H) 4.20 (d, J=14.4 Hz, 1H) 7.71 (d, J=5.6 Hz, 1H) 7.14-7.21 (m, 1H) 7.42-7.48 (dd J=8.8, 4.3 Hz 1H) 7.61-7.65 (m, 3H) 7.69-7.74 (m, 2H). MS [m+H] calc'd C26H29FN5O3 478; found 478.

Provenance & Evidence