HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21625915, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 1,3-Cyclohexanedione | HCID 10434 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21625915 | HCID 21625915 | — |
Reaction Steps
Equimolar amounts of isopropylamine and cyclohexane-1,3-dione were dissolved in benzene and heated with addition of p-toluenesulfonic acid to boiling with a water trap. After the trapping of water was complete, the mixture was thoroughly washed with water, the solvent was stripped off, and the residue was recrystallized.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133913B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-ac0f7555fe6f4429b5f50d42b7233143 |
| Source note | uspto-grants-2012_03 |