Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1094334Generated: November 1, 2026

Water → HCID 21625915, compound

https://huagongshe.com/reaction/1094334

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
Reactantp-Toluenesulfonic acidHCID 6101—
ReactantIsopropylamineHCID 6363—
Reactant1,3-CyclohexanedioneHCID 10434—
SolventBenzeneHCID 241—
ProductHCID 21625915HCID 21625915—

Reaction Steps

Equimolar amounts of isopropylamine and cyclohexane-1,3-dione were dissolved in benzene and heated with addition of p-toluenesulfonic acid to boiling with a water trap. After the trapping of water was complete, the mixture was thoroughly washed with water, the solvent was stripped off, and the residue was recrystallized.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08133913B2
Source datasetuspto-grants-2012_03
ORD IDord-ac0f7555fe6f4429b5f50d42b7233143
Source noteuspto-grants-2012_03