HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluidine → HCID 58007505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluidine | HCID 7813 | — |
| Reactant | 3-Pyridineacetonitrile, 6-(trifluoromethyl)- | HCID 50851127 | — |
| Product | HCID 58007505 | HCID 58007505 | 50.3% |
Reaction Steps
In analogy to example 9, step 1, 4-methylaniline (298 mg, 2.78 mmol) was coupled to (6-trifluoromethyl-pyridin-3-yl)-acetonitrile (750 mg, 4.03 mmol) to provide the title compound as a pale yellow oil (392 mg, 35%) MS m/e: 281.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133909B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-8cb1eeb806b34297a85d6b90126c6bc6 |
| Source note | uspto-grants-2012_03 |