HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 57582356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 1-Bromo-3-methoxypropane | HCID 524551 | — |
| Reactant | 2-Bromo-4-fluorophenol | HCID 605472 | — |
| Product | HCID 57582356 | HCID 57582356 | 88% |
Reaction Steps
2-Bromo-4-fluorophenol (950 mg, 4.97 mmol) and 1-bromo-3-methoxypropane (1000 mg, 6.53 mmol) in acetonitrile (10 ml) was treated as for preparation 62 to afford crude title compound as a yellow oil (1.16 g, 88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134007B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-242bc349ebce49e0bde6b0a4f70f5558 |
| Source note | uspto-grants-2012_03 |