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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1094928Generated: November 1, 2026

HCID 57421777, compound → HCID 57421778, compound

https://huagongshe.com/reaction/1094928

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57421777HCID 57421777—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 57421778HCID 57421778100.8%

Reaction Steps

Methyl 4-(2-tert-butoxycarbonyl-1-hydroxyethyl)benzoate (140 mg, 0.50 mmol) was dissolved in trifluoroacetic acid (2.0 mL), and the resulting solution was left to stand at room temperature for 3 hours and concentrated to dryness under reduced pressure to give 113 mg of the desired product (stoichiometric yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08134013B2
Source datasetuspto-grants-2012_03
ORD IDord-6fca4c6454be46d18bb85cd89104ab1b
Source noteuspto-grants-2012_03