HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57421777, compound → HCID 57421778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57421777 | HCID 57421777 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57421778 | HCID 57421778 | 100.8% |
Reaction Steps
Methyl 4-(2-tert-butoxycarbonyl-1-hydroxyethyl)benzoate (140 mg, 0.50 mmol) was dissolved in trifluoroacetic acid (2.0 mL), and the resulting solution was left to stand at room temperature for 3 hours and concentrated to dryness under reduced pressure to give 113 mg of the desired product (stoichiometric yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134013B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-6fca4c6454be46d18bb85cd89104ab1b |
| Source note | uspto-grants-2012_03 |