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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1094940Generated: October 31, 2026

HCID 86630488, compound → HCID 76597821, compound

https://huagongshe.com/reaction/1094940

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86630488HCID 86630488—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 76597821HCID 7659782156%

Reaction Steps

t-Butyl 3-(5-{1-[4-Hydroxy-5-(4-trifluoromethylphenyl)thiophen-3-yl]ethylidenehydrazinocarbonyl}-N-methylthiophene-2-carboxamido)propionate (30 mg, 0.05 mmol) was stirred with trifluoroacetic acid (300 μL) at room temperature for 15 minutes. The reaction solution was concentrated, and after addition of ether the resulting solid was collected by filtration to give the desired product (yield 56%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08134013B2
Source datasetuspto-grants-2012_03
ORD IDord-068bef0487fd49e29c7770d5d19970c5
Source noteuspto-grants-2012_03