Piperidine → HCID 86666422, compound

HRID 1095012Notes

Reaction equation

HRID 1095012 reaction equation
[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].CS[C:8]1[N:9]([CH3:18])[C:10]2[CH:17]=[CH:16][CH:15]=[CH:14][C:11]=2[N+:12]=1[CH3:13].[NH:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>O1CCOCC1>[Cl:1]([O-:5])(=[O:4])(=[O:3])=[O:2].[NH:19]1[CH2:24][CH2:23][CH2:22][CH2:21][CH:20]1[C:8]1[N:9]([CH3:18])[C:10]2[CH:17]=[CH:16][CH:15]=[CH:14][C:11]=2[N+:12]=1[CH3:13]

Participants

4

Reactant 2

HCID 8082PiperidineHCID 14222620HCID 14222620, compound

Product 1

HCID 86666422HCID 86666422, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Heat 0.01 mol of 2-methylmercapto-1,3-dimethylbenzimidazolium perchlorate with 0.01 mol of piperidine for 4 h at reflux in 250 ml of dioxane. Remove the solids by suction and recrystallise from ethanol.

Workup

  1. customRemove the solids by suction
  2. customrecrystallise from ethanol

Sources & evidence

ORD record
ord-b6138e431ef64544a1885429db8677e7
Source dataset
uspto-grants-2012_03
Patent number
US08134146B2

Reaction notes

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