HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenol → HCID 57743255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Fluoro-5-iodobenzaldehyde | HCID 16217058 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 57743255 | HCID 57743255 | 66% |
Reaction Steps
In a manner similar to the method described in Example 50a, 2-fluoro-5-iodobenzaldehyde (1.2 g, 4.8 mmol) (Aldrich) was reacted with 4-methoxyphenol (0.71 g, 5.76 mmol) and K2CO3 in N,N-dimethylacetamide to give 5-iodo-2-(4-methoxy-phenoxy)-benzaldehyde as a yellow oil (Yield 1.12 g, 66%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134001B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-c58583b6d6b64f41ac77f7c2e9617af4 |
| Source note | uspto-grants-2012_03 |