HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzaldehyde → HCID 28604100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzaldehyde | HCID 6737 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 28604100 | HCID 28604100 | 81.2% |
Reaction Steps
In a manner similar to the method described in Example 50a, 2,6-dichlorobenzaldehyde (2.7 g, 15 mmol) (Aldrich) was reacted with 4-methoxyphenol (1.8 g, 15 mmol) and K2CO3 in N,N-dimethylacetamide to give 2-chloro-6-(4-methoxy-phenoxy)-benzaldehyde as a yellow oil (Yield 3.2 g, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134001B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-c9c5beb95a1346c3b6376d28f808160b |
| Source note | uspto-grants-2012_03 |