HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 178455370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | HCID 178521614 | HCID 178521614 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178455370 | HCID 178455370 | 31.6% |
Reaction Steps
In a manner similar to the method described in example 94a, cis-1,4-cyclohexanediol (3.8 g, 33 mmol) was reacted with tert-butyldimethylchlorosilane (5 g, 34 mmol) and imidazole in N,N-dimethylformamide to give cis-4-(tert-buyl-dimethyl-silanyloxy)-cyclohexanol as a colorless oil (2.4 g, 31%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134001B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-c57b4f90c1b648828e214db1355b1e68 |
| Source note | uspto-grants-2012_03 |