反应详情

In a manner similar to the method described in example 94a, cis-1,4-cyclohexanediol (3.8 g, 33 mmol) was reacted with tert-butyldimethylchlorosilane (5 g, 34 mmol) and imidazole in N,N-dimethylformamide to give cis-4-(tert-buyl-dimethyl-silanyloxy)-cyclohexanol as a colorless oil (2.4 g, 31%).