HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57743258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Fluorosalicylaldehyde | HCID 2737328 | — |
| Reactant | Oxan-4-yl methanesulfonate | HCID 11344352 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57743258 | HCID 57743258 | — |
Reaction Steps
In a manner similar to the method described in Example 4a, 5-fluoro salicylaldehyde (Aldrich) reacted with methanesulfonic acid tetrahydro-pyran-4-yl ester (Example 32a) and potassium carbonate in dimethylformamide to give a solid. MS (H+), 225.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134001B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-aa629a5f62184a9ea2080a3f92e37679 |
| Source note | uspto-grants-2012_03 |