4-Methoxyphenol → HCID 43313276, compound

HRID 1095197Notes

Reaction equation

HRID 1095197 reaction equation
[F:1][C:2]1[CH:9]=[C:8](F)[CH:7]=[CH:6][C:3]=1C=O.[CH3:11][O:12][C:13]1[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][CH:14]=1.[C:20](=[O:23])([O-])[O-].[K+].[K+]>>[CH3:11][O:12][C:13]1[CH:18]=[CH:17][C:16]([O:19][C:7]2[CH:8]=[CH:9][C:2]([F:1])=[CH:3][C:6]=2[CH:20]=[O:23])=[CH:15][CH:14]=1

Participants

4

Reactant 3

HCID 90154-MethoxyphenolHCID 11430Potassium CarbonateHCID 737702,4-Difluorobenzaldehyde

Product 1

HCID 43313276HCID 43313276, compound

Procedure

In a similar manner to the method described in Example 140a, 2,4-difluoro-benzaldehyde (Aldrich) was reacted with 4-methoxy-phenol and potassium carbonate to give a solid. MS (H+), 247.

Workup

  1. customto give a solid

Sources & evidence

ORD record
ord-5476c718d8954b379fb92753fedb3e73
Source dataset
uspto-grants-2012_03
Patent number
US08134001B2

Reaction notes

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