HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66782075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86628971 | HCID 86628971 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Solvent | Ether isohexane | HCID 21882825 | — |
| Product | HCID 66782075 | HCID 66782075 | — |
Reaction Steps
The product from step (i) (1.1 g) was dissolved in methanol/DCM (1/1, 40 ml). 4N—HCl in dioxane (10 ml) was added and the mixture stirred at rt for 20 h. The resultant was concentrated under reduced pressure, which afforded the subtitle compound. Yield 0.9 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138172B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-68a4b9e0fbf94b55ab3cabb364b98ebb |
| Source note | uspto-grants-2012_03 |