HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 59492371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 24961699 | HCID 24961699 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59492371 | HCID 59492371 | — |
Reaction Steps
The product from example 12 (150 mg) was dissolved in DCM (10 ml) and methanol (2 ml) and mCPBA (0.1 g) added. The mixture was stirred at rt for 3 h then purified by RPHPLC, which afforded the title compound. Yield 50 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138172B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-cdbe42fc07804aa38ca1fae758f6fb8f |
| Source note | uspto-grants-2012_03 |