Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1095337Generated: October 30, 2026

Trifluoroacetic acid → HCID 24962427, compound

https://huagongshe.com/reaction/1095337

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86645626HCID 86645626—
SolventDichloromethaneHCID 6344—
ProductHCID 24962427HCID 24962427—

Reaction Steps

The product from example 20 step (i) (100 mg) was dissolved in DCM (1 ml) and TFA (0.2 ml) added. The mixture was stirred at rt for 2 h. The solution was washed with saturated aqueous NaHCO3 and dried. The mixture was purified by RPHPLC, which afforded the title compound. Yield 30 mg

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08138172B2
Source datasetuspto-grants-2012_03
ORD IDord-81509696744a4faea8f84c0e73108740
Source noteuspto-grants-2012_03