HRID1095337

反应详情

EQUATION

反应方程式

HRID 1095337 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The product from example 20 step (i) (100 mg) was dissolved in DCM (1 ml) and TFA (0.2 ml) added. The mixture was stirred at rt for 2 h. The solution was washed with saturated aqueous NaHCO3 and dried. The mixture was purified by RPHPLC, which afforded the title compound. Yield 30 mg

WORKUP

后处理

  1. washThe solution was washed with saturated aqueous NaHCO3
  2. customdried
  3. customThe mixture was purified by RPHPLC, which