HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide dichloromethane → HCID 66783669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide dichloromethane | HCID 22277759 | — |
| Reactant | HCID 66783822 | HCID 66783822 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 66783669 | HCID 66783669 | 28% |
Reaction Steps
The methoxy compound (1.15 g, 3.39 mmol) obtained in (a) was dissolved in chloroform, and processed with 1.0 M boron tribromide/dichloromethane solution (11 ml, 11 mmol) at 0° C. according to the same method as in Example 5-(b) or according to a method similar to it, thereby obtaining the entitled compound as a crude product (308 mg, 28%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138206B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-ca2215e07f2743299ad7fefedacb1b59 |
| Source note | uspto-grants-2012_03 |