Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1095827Generated: November 3, 2026

Boron tribromide dichloromethane → HCID 66783669, compound

https://huagongshe.com/reaction/1095827

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBoron tribromide dichloromethaneHCID 22277759—
ReactantHCID 66783822HCID 66783822—
SolventChloroformHCID 6212—
ProductHCID 66783669HCID 6678366928%

Reaction Steps

The methoxy compound (1.15 g, 3.39 mmol) obtained in (a) was dissolved in chloroform, and processed with 1.0 M boron tribromide/dichloromethane solution (11 ml, 11 mmol) at 0° C. according to the same method as in Example 5-(b) or according to a method similar to it, thereby obtaining the entitled compound as a crude product (308 mg, 28%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08138206B2
Source datasetuspto-grants-2012_03
ORD IDord-ca2215e07f2743299ad7fefedacb1b59
Source noteuspto-grants-2012_03