HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 66699206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 66699404 | HCID 66699404 | — |
| Product | HCID 66699206 | HCID 66699206 | — |
Reaction Steps
In analogy to Example 147, step 5, 3-chloro-5-[2-(2-chloro-4-methoxy-phenyl)-1-hydroxy-1-trifluoromethyl-propyl]-1-methyl-1H-pyridin-2-one was reacted with BBr3 to give the title compound as an off-white solid. MS (m/e, ISP neg. ion)=393.8 [M−H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138189B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-32d2bd4f4f6a4059b2233d73940f52e1 |
| Source note | uspto-grants-2012_03 |