HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1,2-dichloro-4-iodo- → 1-(3,4-Dichloro-phenyl)-4-(3-piperidin-1-yl-propyl)-[1,4]diazepan-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1,2-dichloro-4-iodo- | HCID 88591 | — |
| Reactant | 4-(3-Piperidin-1-yl-propyl)-[1,4]diazepan-5-one | HCID 66783026 | — |
| Product | 1-(3,4-Dichloro-phenyl)-4-(3-piperidin-1-yl-propyl)-[1,4]diazepan-5-one | HCID 59159245 | — |
Reaction Steps
The title compound was prepared from 4-(3-piperidin-1-yl-propyl)-[1,4]diazepan-5-one (Example 33B) and 1,2-dichloro-4-iodo-benzene in analogy to example 33. MS: 384.4 (MH+, 2Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138175B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-346a4666b1af42bbaadd6a88ae16127f |
| Source note | uspto-grants-2012_03 |