3,5-Dimethylbenzenesulfonyl chloride → HCID 66786290, compound

Participants

Reaction Steps

The title compound was prepared from tert-butyl 1,3,4,6-tetrahydro-5H-azepino[5,4,3-cd]indole-5-carboxylate, Intermediate 12 (14 mg, 0.05 mmol) and 3,5-dimethylbenzenesulfonyl chloride (15 mg, 0.75 mmol) as described in the general procedure above, to give 8.9 mg of product. MS (ESI) m/z 341 [M+H]+.

Provenance & Evidence