反应详情

Prepared from 3-chloro-2-methylbenzoic acid (4.80 g, 28.1 mmol) and cyclopropylamine according to above-described procedures C and E (5.50 g, quantitative over 2 steps). LC-MS (3-chloro-N-cyclopropyl-2-methylbenzamide): tR=0.81 min, ES+: 210.11; LC-MS (title compound): tR=0.62 min, ES+: 196.05.