HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 66783580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | 2-Chloro-3-fluorobenzoic acid | HCID 302620 | — |
| Product | HCID 66783580 | HCID 66783580 | — |
Reaction Steps
Prepared from 2-chloro-3-fluorobenzoic acid (2.00 g, 11.5 mmol) and cyclopropylamine according to above-described procedures C and E, and purified over amberlyst A15 (1.86 g, 81% over 2 steps). LC-MS (2-chloro-N-cyclopropyl-3-fluorobenzamide): tR=0.76 min, ES+: 214.10; LC-MS (title compound): tR=0.60 min, ES+: 200.12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138340B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-855e8c4768f44a2b9b8e9f09da936a67 |
| Source note | uspto-grants-2012_03 |