HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1097005Generated: October 27, 2026
Hydrochloric Acid → HCID 178434226, compound
https://huagongshe.com/reaction/1097005
Participants
| Role | Name | HCID | Charge |
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| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-(5-Bromo-3-methyl-1H-indazol-1-yl)ethan-1-one | HCID 59127382 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178434226 | HCID 178434226 | — |
Reaction Steps
1-Acetyl-5-bromo-3-methyl-1H-indazole (1.23 g) was added to the solution of hydrochloride in methanol (30 ml), and stirred for 30 min at 60° C. The mixture was concentrated under reduced pressure, and the residue was crystallized from mixed solvent of hexane and EtOAc to give the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08138197B2 |
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| Source dataset | uspto-grants-2012_03 |
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| ORD ID | ord-2a8746bc7f0f4de9985697c071cabdf6 |
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| Source note | uspto-grants-2012_03 |
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