HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 57930912, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 57930904 | HCID 57930904 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57930912 | HCID 57930912 | — |
Reaction Steps
To a solution of Methyl 4-(1-cyclopropyl-1H-pyrazol-4-yl)-3,5-diethoxybenzoate (20 mg) in MeOH (3 ml) was added aqueous 1N NaOH (240 ul) at room temperature, and the reaction mixture was stirred for over night. The mixture was concentrated under reduced pressure and aqueous 1N HCl (240 ul) was added to the residue. The mixture was concentrated under reduced pressure and dried in vacuo to give the crude title compound which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138197B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-a19894d213a3476abbb7802429bdba40 |
| Source note | uspto-grants-2012_03 |