HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178420353, compound → HCID 178511580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178420353 | HCID 178420353 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178511580 | HCID 178511580 | — |
Reaction Steps
7.2 g (16.4 mmol) of trans-dibenzyl-4-morpholino-cyclohexylamine are dissolved in 100 mL of MeOH and hydrogenated on 1.4 g of Pd/C (10%) at 30-50° C. The solvent is eliminated in vacuo and the residue is crystallised from ethanol and concentrated HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143247B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-ebc29fad280c407d8638f9ce4b4345c7 |
| Source note | uspto-grants-2012_03 |