HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24765764, compound → 5-Ethyl-1-propyl-5-(4,5,6,7-tetrafluoro-1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-2,4,6(1H,3H,5H)-pyrimidinetrione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24765764 | HCID 24765764 | — |
| Reactant | HCID 66811200 | HCID 66811200 | — |
| Product | 5-Ethyl-1-propyl-5-(4,5,6,7-tetrafluoro-1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-2,4,6(1H,3H,5H)-pyrimidinetrione | HCID 24765667 | — |
Reaction Steps
Compound 19e was synthesized in the same manner as described for 19a from 5-amino-5-ethyl-1-propylbarbituric acid hydrochloride (0.38 g, 1.50 mmol). The crude product was recrystallized from EtOH (70%) to give 5-ethyl-1-propyl-5-(tetrafluorophthalimido)-barbituric acid (19e) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143252B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-12774bce4aa8473bb928f028b110f61d |
| Source note | uspto-grants-2012_03 |