HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178508255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 178514143 | HCID 178514143 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178508255 | HCID 178508255 | — |
Reaction Steps
The product of example 1 step a) (7.35 g) was heated at 120° C. in N,N-dimethylformamide (40 ml)/water (10 ml) for 10 hours. After cooling, the resulting solid was filtered off, washed with water, then ethyl acetate to give the subtitle compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143261B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-edc8f84e772f4cd7b6442348ad29fbf1 |
| Source note | uspto-grants-2012_03 |