反应详情

温度

60 °C

To a solution of the product from example 1 step d) (0.1 g) in bromoform (5 ml) was added isoamylnitrite (0.13 ml) and the mixture heated at 60° C. for 10 mins. The mixture was evaporated to dryness and purified (SiO2, ethyl acetate:dichloromethane 1:9 as eluant) to give the subtitle compound as a colourless solid (0.043 g).

1. customThe mixture was evaporated to dryness
2. custompurified (SiO2, ethyl acetate:dichloromethane 1:9 as eluant)