2-(2-chloro-4-formylphenoxy)acetamide → HCID 22671343, compound

Participants

Reaction Steps

To a solution of the product from example 15 step a) (4.4 g) in ethanol (500 ml) was added sodium borohydride (1.56 g) and the mixture allowed to stir for 1 hour. Acidified with glacial acetic acid, evaporated to dryness and extracted into ethyl acetate, washed with water to give the subtitle compound (4.3 g).

Provenance & Evidence