HRID10974

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11166

3-Iodo-1-propene

C3H5I

结构：CC(C)(C)OC(=O)[C@@H]1CCc2ncc(NC(=O)OCc3ccccc3)c(=O)n21

HCID54224046

未命名化合物

结构：CC(C)(C)OC(=O)C1(C)CCc2ncc(NC(=O)OCc3ccccc3)c(=O)n21

HCID69600879

未命名化合物

PRODUCTS

生成物

结构：C=CCC1(C(=O)OC(C)(C)C)CCc2ncc(NC(=O)OCc3ccccc3)c(=O)n21

HCID69600950

未命名化合物

收率 55%

PROCEDURE

实验过程

According to the procedure for the preparation of intermediate 19a, alkylation of intermediate 1g (250 mg, 0.649 mmol) with allyl iodide afforded 153 mg (55%) of intermediate 20a. MS (ESI) 426.4 (M+H+), 448.4 (M+Na+).