HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → HCID 57438628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | 2-Amino-5-methylpyridine | HCID 15348 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Product | HCID 57438628 | HCID 57438628 | — |
Reaction Steps
The title compound was prepared in a manner similar to that described for Intermediate A16 and Intermediate A2 (Step 2-Step 3) starting from diethyl malonate, 2-bromoethyl methyl ether and 2-amino-5-picoline, 1H NMR (300 MHz, CDCl3) δ 9.24 (br s, 1H), 8.14 (m, 2H), 7.52 (dd, 1H), 4.48 (br s, 1H), 4.39 (m, 1H), 3.69 (m, 2H), 3.39 (s, 3H), 2.25 (m, 4H), 2.09 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143263B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-18942a8ddedb497aa11c1cd81af09eea |
| Source note | uspto-grants-2012_03 |