反应详情

To S-1-(4-fluorophenyl)-1H-indazol-5-yl benzothioate (0.046 g, 0.13 mmol) in methanol (3 mL), potassium carbonate (0.011 mL, 0.20 mmol) was added and the mixture was stirred at r.t. for 2 h. water was than added, 1N HCl (2 ml) and extracted with EtOAc (2*20 ml), dried, evaporated and then purified on HPLC. The relevant fractions were collected freeze dried and analysed by LC/MS.

1. additionthan added
2. extraction1N HCl (2 ml) and extracted with EtOAc (2*20 ml)
3. customdried
4. customevaporated
5. custompurified on HPLC
6. customThe relevant fractions were collected freeze
7. customdried