HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 59339623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 59339877 | HCID 59339877 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59339623 | HCID 59339623 | — |
Reaction Steps
To a stirred solution of (R)-t-butyl 1-(3-methoxy-4-(methylthio)phenyl)-1-oxopropan-2-ylcarbamate (308d, 55 μg, 170 μmol) in THF (2 mL) at r.t. was added sodium tetrahydroborate (48 μg, 1.27 mmol) in small portions, and the mixture was stirred for 3 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143290B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-4ce661f49423428f8051fdec38677d72 |
| Source note | uspto-grants-2012_03 |