HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 57911433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 57911441 | HCID 57911441 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57911433 | HCID 57911433 | — |
Reaction Steps
TBAF (1.041 mL, 1.041 mmol) was added to the THF (5 mL) solution of (E)-6-phenyl-9-(triisopropylsilyloxy)-8,9-dihydro-7H-cyclohepta[b]pyridine (0.2049 g, 0.521 mmol) at rt. The reaction was stirred at room temperature for 6 hours. The solvent was removed via vacuum to give the crude product. MS (ESI)[M+H+]=238.25.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143403B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-24d656705f7f4fb1ab1ce762edf93259 |
| Source note | uspto-grants-2012_03 |