HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1-methyl-1H-imidazol-2-yl)methanol → HCID 59354906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1-methyl-1H-imidazol-2-yl)methanol | HCID 573612 | — |
| Reactant | Ethyl 6-chloronicotinate | HCID 2799611 | — |
| Product | HCID 59354906 | HCID 59354906 | 46% |
Reaction Steps
The title compound was synthesized as described for Intermediate example I-92 in 46% yield starting from ethyl 6-chloronicotinate and (1-methyl-1h-imidazol-2-yl)methanol; 1H NMR (400 MHz, DMSO-d6) δ ppm 8.74 (d, 1 H), 8.24 (dd, 1 H), 7.58-7.74 (m, 2 H), 7.06 (d, 1 H), 5.69 (s, 2 H), 3.92 (s, 3 H); MS (APPI/APCI) m/z 234[M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143408B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-913445e61ecb41819dc4ebd404351597 |
| Source note | uspto-grants-2012_03 |