Iodine I-131 → HCID 59354918, compound

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Reaction Steps

The title compound was synthesized as described for Intermediate example I-131 in 54% yield starting from ethyl 5-methyl-2H-1,2,3-triazole-4-carboxylate and 2-bromoethyl methyl ether; 1H NMR (400 MHz, CDCl3) δ ppm 4.58 (t, 2 H), 4.42 (q, 2 H), 3.90 (t, 2 H), 3.35 (s, 3 H), 2.49-2.56 (m, 3 H), 1.34-1.46 (m, 3 H); MS (ESI) m/z 214[M+H+].

Provenance & Evidence